Presenter Information

Cole SchliepFollow

Location

Student Center

Document Type

Poster

Start Date

19-8-2025 2:30 PM

End Date

19-8-2025 3:30 PM

Description

Tröger’s base is a unique V-shaped, bicyclic, chiral molecule that has the flexibility to have derivatives added to its carbon backbone. This allows for Tröger’s base to be used in many material applications. This research focuses on the addition of a carbamoyl group(-CONEt2) to Tröger’s base that can form either an endo- or exo-isomeric form. The exo-derivative of Tröger’s base is shown to be the more stable species. Recent work has shown that the endo-derivative can be selectively produced by sequential proton transfer under highly-basic, cold conditions, through deprotonation followed by a protic quench. Prior research has predicted that this reaction proceeds through a charged enolate intermediate, but has not shown a clear mechanism for selectivity of the endo-product. This project focused on determining the impact of the THF solvent and the effect temperature has on both mechanistic steps using Density Functional Theory (DFT) calculations.

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Aug 19th, 2:30 PM Aug 19th, 3:30 PM

Determination of the Reaction Mechanism for the Tautomerization of Tröger’s Base

Student Center

Tröger’s base is a unique V-shaped, bicyclic, chiral molecule that has the flexibility to have derivatives added to its carbon backbone. This allows for Tröger’s base to be used in many material applications. This research focuses on the addition of a carbamoyl group(-CONEt2) to Tröger’s base that can form either an endo- or exo-isomeric form. The exo-derivative of Tröger’s base is shown to be the more stable species. Recent work has shown that the endo-derivative can be selectively produced by sequential proton transfer under highly-basic, cold conditions, through deprotonation followed by a protic quench. Prior research has predicted that this reaction proceeds through a charged enolate intermediate, but has not shown a clear mechanism for selectivity of the endo-product. This project focused on determining the impact of the THF solvent and the effect temperature has on both mechanistic steps using Density Functional Theory (DFT) calculations.